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Analysis of physical properties of gas hydrate-bearing unconsolidated sediment samples from the ultra-deepwater

《能源前沿（英文）》 2022年 第16卷 第3期   页码 509-520 doi: 10.1007/s11708-021-0786-4

摘要： Marine natural gas hydrate has recently attracted global attention as a potential new clean energy source. Laboratory measurements of various physical properties of gas hydrate-bearing marine sediments can provide valuable information for developing efficient and safe extraction technology of natural gas hydrates. This study presents comprehensive measurement results and analysis of drilled hydrate-bearing sediments samples recovered from Qiongdongnan Basin in the South China Sea. The results show that the gas hydrate in the core samples is mainly methane hydrate with a methane content of approximately 95%, and the other components are ethane and carbon dioxide. The saturation of the samples fluctuates from 2%–60%, the porosity is approximately 38%–43%, and the water content is approximately 30%–50%, which indicate that high water saturation means that timely drainage should be paid attention to during hydrate extraction. In addition, the median diameter of the sediment samples is mainly distributed in the range of 15 to 34 μm, and attention should be paid to the prevention and control of sand production in the mining process. Moreover, the thermal conductivity is distributed in the range of 0.75 to 0.96 W/(m∙K) as measured by the flat plate heat source method. The relatively low thermal conductivity of hydrates at this study site indicates that a combined approach is encouraged for natural gas production technologies. It is also found that clay flakes and fine particles are attached to the surface of large particles in large numbers. Such characteristics will lead to insufficient permeability during the production process.

关键词： natural gas hydrates     physical properties analysis     hydrate-bearing sediments    

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Fundamental characteristics of gas hydrate-bearing sediments in the Shenhu area, South China Sea

Xin LYU, Qingping LI, Yang GE, Junlong ZHU, Shouwei ZHOU, Qiang FU

《能源前沿（英文）》 2021年 第15卷 第2期   页码 367-373 doi: 10.1007/s11708-020-0714-z

摘要： The basic physical properties of marine natural gas hydrate deposits are important to the understanding of seabed growth conditions, occurrence regularity, and occurrence environment of natural gas hydrates. A comprehensive analysis of the core samples of drilling pressure-holding hydrate deposits at a depth of 1310 m in the Shenhu area of the South China Sea was conducted. The experimental results indicate that the particle size in the hydrate sediment samples are mainly distributed in the range from 7.81 µm to 21.72µm, and the average particle size decreases as the depth of the burial increases. The X-ray CT analytical images and surface characteristics SEM scan images suggest that the sediment is mostly silty clay. There are a large number of bioplastics in the sediment, and the crack inside the core may be areas of hydrate formation.

关键词： natural gas hydrate     Shenhu area     reservoirs characteristics    

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Research progress on hydrate plugging in multiphase mixed rich-liquid transportation pipelines

Shuyu SONG, Zhiming LIU, Li ZHOU, Liyan SHANG, Yaxin WANG

《能源前沿（英文）》 2022年 第16卷 第5期   页码 774-792 doi: 10.1007/s11708-020-0688-x

摘要： The plugging mechanism of multiphase mixed rich-liquid transportation in submarine pipeline is a prerequisite for maintaining the fluid flow in the pipeline and ensuring safe fluid flow. This paper introduced the common experimental devices used to study multiphase flow, and summarized the plugging progress and mechanism in the liquid-rich system. Besides, it divided the rich-liquid phase system into an oil-based system, a partially dispersed system, and a water-based system according to the different water cuts, and discussed the mechanism of hydrate plugging. Moreover, it summarized the mechanism and the use of anti-agglomerates in different systems. Furthermore, it proposed some suggestions for future research on hydrate plugging. First, in the oil-based system, the effect factors of hydrates are combined with the mechanical properties of hydrate deposit layer, and the hydrate plugging mechanism models at inclined and elbow pipes should be established. Second, the mechanism of oil-water emulsion breaking in partially dispersed system and the reason for the migration of the oil-water interface should be analyzed, and the property of the free water layer on the hydrate plugging process should be quantified. Third, a complete model of the effect of the synergy of liquid bridge force and van der Waals force in the water-based system on the hydrate particle coalescence frequency model is needed, and the coalescence frequency model should be summarized. Next, the dynamic analysis of a multiphase mixed rich-liquid transportation pipeline should be coupled with the process of hydrate coalescence, deposition, and blockage decomposition. Finally, the effects of anti-agglomerates on the morphological evolution of hydrate under different systems and pipeline plugging conditions in different media should be further explored.

关键词： hydrate     rich-liquid phase     plugging mechanism     coalescence     deposition     anti-agglomerate    

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Adsorption and partition of benzo(a)pyrene on sediments with different particle sizes from the Yellow

XIA Xinghui, HU Lijuan, MENG Lihong

《环境科学与工程前沿（英文）》 2007年 第1卷 第2期   页码 172-178 doi: 10.1007/s11783-007-0030-4

摘要： Experiments have been carried out to study the sorption of Benzo(a)pyrene(Bap) on sediment particles from the Yellow River using a batch equilibration technique. Effects of particle size on the adsorption and partition of Bap were investigated with the particle content of 3 g/L. Several significant results were obtained from the study. (1) Isotherms of Bap could be fitted with the dual adsorption-partition model under different particle sizes, and the measured value of the adsorption and partition was in agreement with the theoretical value of the dual adsorption-partition model. (2) When the particle diameter was "e 0.025 mm, the adsorption was predominant in the sorption of Bap, which accounted for 68.7% 82.4% of the sorption. For the particles with the size of 0.007 mm "e < 0.025 mm, the adsorption was predominant when the equilibrium concentration of Bap was 0 8.87 μg/L in the water phase; and the partition was predominant when the equilibrium concentration of Bap was higher than 8.87 μg/L in the water phase. When the particle diameter was <0.007 mm, the partition was predominant. (3) On the point of particle size, the contribution of adsorption to sorption followed the order: "e0.025 mm > 0.007 mm "d<0.025 mm > <0.007 mm . (4) The partition coefficients of Bap in solids with different particle sizes were linearly correlated with the organic content, and the K of Bap was about 1.26 x 10 (L/kg).
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Prediction of bed load sediments using different artificial neural network models

Reza ASHEGHI, Seyed Abbas HOSSEINI

《结构与土木工程前沿（英文）》 2020年 第14卷 第2期   页码 374-386 doi: 10.1007/s11709-019-0600-0

摘要： Modeling and prediction of bed loads is an important but difficult issue in river engineering. The introduced empirical equations due to restricted applicability even in similar conditions provide different accuracies with each other and measured data. In this paper, three different artificial neural networks (ANNs) including multilayer percepterons, radial based function (RBF), and generalized feed forward neural network using five dominant parameters of bed load transport formulas for the Main Fork Red River in Idaho-USA were developed. The optimum models were found through 102 data sets of flow discharge, flow velocity, water surface slopes, flow depth, and mean grain size. The deficiency of empirical equations for this river by conducted comparison between measured and predicted values was approved where the ANN models presented more consistence and closer estimation to observed data. The coefficient of determination between measured and predicted values for empirical equations varied from 0.10 to 0.21 against the 0.93 to 0.98 in ANN models. The accuracy performance of all models was evaluated and interpreted using different statistical error criteria, analytical graphs and confusion matrixes. Although the ANN models predicted compatible outputs but the RBF with 79% correct classification rate corresponding to 0.191 network error was outperform than others.

关键词： bed load prediction     artificial neural network     modeling     empirical equations    

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Progress in use of surfactant in nearly static conditions in natural gas hydrate formation

Zhen PAN, Yi WU, Liyan SHANG, Li ZHOU, Zhien ZHANG

《能源前沿（英文）》 2020年 第14卷 第3期   页码 463-481 doi: 10.1007/s11708-020-0675-2

摘要： Natural gas hydrate is an alternative energy source with a great potential for development. The addition of surfactants has been found to have practical implications on the acceleration of hydrate formation in the industrial sector. In this paper, the mechanisms of different surfactants that have been reported to promote hydrate formation are summarized. Besides, the factors influencing surfactant-promoted hydrate formation, including the type, concentration, and structure of the surfactant, are also described. Moreover, the effects of surfactants on the formation of hydrate in pure water, brine, porous media, and systems containing multiple surfactants are discussed. The synergistic or inhibitory effects of the combinations of these additives are also analyzed. Furthermore, the process of establishing kinetic and thermodynamic models to simulate the factors affecting the formation of hydrate in surfactant-containing solutions is illustrated and summarized.

关键词： gas hydrate     kinetic hydrate promoter     compounding     model     surfactant     mechanism    

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Sorption of tetracycline to sediments and soils: assessing the roles of pH, the presence of cadmium andproperties of sediments and soils

Guixiang ZHANG, Xitao LIU, Ke SUN, Ye ZHAO, Chunye LIN

《环境科学与工程前沿（英文）》 2010年 第4卷 第4期   页码 421-429 doi: 10.1007/s11783-010-0265-3

摘要： Batch sorption experiments were conducted to evaluate the sorption behavior of tetracycline (TC, H L) on sediments and soils in the presence and absence of cadmium (Cd), as affected by pH and properties of sediments and soils. The results indicated stronger nonlinearity and higher capacity of TC sorption on sediments than on soils. Sorption of TC also strongly depended on environmental factors and sediment/soil properties. Lower pH facilitated TC sorption through a cation exchange mechanism, which also took place at pH values above 5.5, where TC existed as a zwitterion (H L ) or anions (HL and L ). When pH was above 7, however, ligand-promoted dissolution of TC might occur due to TC weakening the Al-O bond of aluminum oxide and the Fe-O bond of iron oxide. Natural organic matter (NOM) plays a more important role in TC sorption than cation exchange capacity (CEC) and clay contents. The presence of Cd (II) increased TC sorption on both sediments and soils, which resulted from the decrease of equilibrium solution pH caused by Cd exchange with H ions of sediment/soil surfaces. The increase of TC sorption was also related to the formation of TC-Cd complexes, where Cd acted as a bridge between the sediment/soil and TC.

关键词： sorption     tetracycline (TC)     pH     cadmium (Cd)     antibiotic    

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Impacts of CO2 and H2S on the risk of hydrate formation during pipeline transport of natural gas

Solomon A. Aromada, Bjørn Kvamme

《化学科学与工程前沿（英文）》 2019年 第13卷 第3期   页码 616-627 doi: 10.1007/s11705-019-1795-2

摘要： Evaluation of maximum content of water in natural gas before water condenses out at a given temperature and pressure is the initial step in hydrate risk analysis during pipeline transport of natural gas. The impacts of CO and H S in natural gas on the maximum mole-fractions of water that can be tolerated during pipeline transport without the risk of hydrate nucleation has been studied using our novel thermodynamic scheme. Troll gas from the North Sea is used as a reference case, it contains very negligible amount of CO and no H S. Varying mole-fractions of CO and H S were introduced into the Troll gas, and the effects these inorganic impurities on the water tolerance of the system were evaluated. It is observed that CO does not cause any distinguishable impact on water tolerance of the system, but H S does. Water tolerance decreases with increase in concentration of H S. The impact of ethane on the system was also investigated. The maximum mole-fraction of water permitted in the gas to ensure prevention of hydrate formation also decreases with increase in the concentration of C H like H S. H S has the most impact, it tolerates the least amount of water among the components studied.

关键词： hydrate     hydrogen Sulphide     CO2     dew point     pipeline    

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in numerical simulations on multiphase flow and thermodynamics in production of natural gas from gas hydrate

Lin ZUO, Lixia SUN, Changfu YOU

《能源前沿（英文）》 2009年 第3卷 第2期   页码 152-159 doi: 10.1007/s11708-009-0017-x

摘要： Natural gas hydrates are promising potential alternative energy resources. Some studies on the multiphase flow and thermodynamics have been conducted to investigate the feasibility of gas production from hydrate dissociation. The methods for natural gas production are analyzed and several models describing the dissociation process are listed and compared. Two prevailing models, one for depressurization and the other for thermal stimulation, are discussed in detail. A comprehensive numerical method considering the multiphase flow and thermodynamics of gas production from various hydrate-bearing reservoirs is required to better understand the dissociation process of natural gas hydrate, which would be of great benefit to its future exploration and exploitation.

关键词： numerical simulation     natural gas hydrate     dissociation     thermodynamics     multiphase flow    

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Efficient promotion of methane hydrate formation and elimination of foam generation using fluorinated

Quan CAO, Dongyan XU, Huanfei XU, Shengjun LUO, Rongbo GUO

《能源前沿（英文）》 2020年 第14卷 第3期   页码 443-451 doi: 10.1007/s11708-020-0683-2

摘要： Methane hydrate preparation is an effective method to store and transport methane. In promoters to facilitate methane hydrate formation, homogeneous surfactant solutions, sodium dodecyl sulfate (SDS) in particular, are more favorable than heterogeneous particles, thanks to their faster reaction rate, more storage capacity, and higher stability. Foaming, however, could not be avoided during hydrate dissociation with the presence of SDS. This paper investigated the ability of five fluorinated surfactants: potassium perfluorobutane sulfonate (PBS), potassium perfluorohexyl sulfonate (PHS), potassium perfluorooctane sulfonate (POS), ammonium perfluorooctane sulfonate (AOS), and tetraethylammonium perfluorooctyl sulfonate (TOS) to promote methane hydrate formation. It was found that both PBS and PHS achieve a storage capacity of 150 ( , the volume of methane that can be stored by one volume of water) within 30 min, more than that of SDS. Cationic ions and the carbon chain length were then discussed on their effects during the formation. It was concluded that PBS, PHS, and POS produced no foam during hydrate dissociation, making them promising promoters in large-scale application.

关键词： methane hydrate     fluorinated surfactants     homogeneous promoter     foam elimination     stability    

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Progress and prospect of hydrate-based desalination technology

Jibao ZHANG, Shujun CHEN, Ning MAO, Tianbiao HE

《能源前沿（英文）》 2022年 第16卷 第3期   页码 445-459 doi: 10.1007/s11708-021-0740-5

摘要： With the continuous growth of the population and the improvement of production, the shortage of freshwater has plagued many countries. The use of novel technologies such as desalination to produce fresh water on a large scale has become inevitable in the world. Hydrate-based desalination (HBD) technology has drawn an increasing amount of attention due to its mild operation condition and environmental friendliness. In this paper, literature on hydrate-based desalination is comprehensively analyzed and critically evaluated, focuses on experimental progress in different hydrate formers that have an impact on thermodynamics and dynamics in hydrate formation. Besides, various porous media promotion is investigated. Besides, the hydrate formation morphology and hydrate crystal structure with different hydrate formers are analyzed and compared. Moreover, molecular dynamic simulation is discussed to further understand microscopic information of hydrate formation. Furthermore, simulations of the HBD process by considering the energy consumption are also investigated. In conclusion, the hydrated based desalination is a potential technology to get fresh water in a sustainable way.

关键词： gas hydrates     desalination     crystal morphology     molecular dynamic     cold energy    

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Assessment on contaminations in sediments of an intake and the inflow canals in Taihu Lake, China

Xiaolong WANG,Shiming DING,Qi ZHANG,Weiping HU

《环境科学与工程前沿（英文）》 2015年 第9卷 第4期   页码 665-674 doi: 10.1007/s11783-014-0701-x

摘要： As the second largest freshwater lake in China, Taihu Lake provides water supply to approximately 32 million inhabitants around the lake. However, dramatically increased pollution has threatened the safety of drinking water supply in recent years. In the present study, we investigated the contaminations of nutrients and heavy metals in the sediments of an intake and inflow canals in Gonghu Bay, Taihu Lake. Moreover, we also examined the impact of human activities on spatial distribution characteristics of contaminations. Our results showed that the intake presented relatively lower concentrations of phosphorus and nitrogen compared with inflow canals. However, the concentrations of Cr, Ni, Cu, Zn and Pb in the sediments of the intake exceeded the lowest effect level (LEL) values, indicating a potential risk to drinking water resource. In addition, the concentrations of Ni in the sediments of Tianji Canal and Jinshu Canal exceeded the severe effect level (SEL) value. More importantly, the concentrations of Cu in the sediments of Tianji Canal exceeded three times of the SEL value. Multivariate statistical analysis confirmed that the domestic sewage primarily contributed to the nutrient accumulation, and the leakage of electronic trash dominated the enrichment of metals in the sediments. Taken together, more effort should be made to ensure the security of water resources in Taihu Lake, especially for the treatment of domestic sewage and industrial wastewater.

关键词： drinking water resource     nutrients     heavy metals     sediments     Taihu Lake    

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Key issues in development of offshore natural gas hydrate

Shouwei ZHOU, Qingping LI, Xin LV, Qiang FU, Junlong ZHU

《能源前沿（英文）》 2020年 第14卷 第3期   页码 433-442 doi: 10.1007/s11708-020-0684-1

摘要： As a new clean energy resource in the 21st century, natural gas hydrate is considered as one of the most promising strategic resources in the future. This paper, based on the research progress in exploitation of natural gas hydrate (NGH) in China and the world, systematically reviewed and discussed the key issues in development of natural gas hydrate. From an exploitation point of view, it is recommended that the concepts of diagenetic hydrate and non-diagenetic hydrate be introduced. The main factors to be considered are whether diagenesis, stability of rock skeleton structure, particle size and cementation mode, thus NGHs are divided into 6 levels and used unused exploitation methods according to different types. The study of the description and quantitative characterization of abundance in hydrate enrichment zone, and looking for gas hydrate dessert areas with commercial exploitation value should be enhanced. The concept of dynamic permeability and characterization of the permeability of NGH by time-varying equations should be established. The ‘Three-gas co-production’ (natural gas hydrate, shallow gas, and conventional gas) may be an effective way to achieve early commercial exploitation. Although great progress has been made in the exploitation of natural gas hydrate, there still exist enormous challenges in basic theory research, production methods, and equipment and operation modes. Only through hard and persistent exploration and innovation can natural gas hydrate be truly commercially developed on a large scale and contribute to sustainable energy supply.

关键词： natural gas hydrate exploitation offshore     diagenetic and non-diagenetic hydrate     solid-state fluidization method     dessert in enrichment area     three-gas combined production on gas hydrate abundance    

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The temporal changes of the concentration level of typical toxic organics in the river sediments around

Qiang Li, Xiong Xu, Yaoyao Fang, Ruiyang Xiao, Donghong Wang, Wenjue Zhong

《环境科学与工程前沿（英文）》 2018年 第12卷 第6期 doi: 10.1007/s11783-018-1054-7

摘要：

The current situation of typical organics in the sediments around Beijing was unclear.

56 kinds of typical toxic organics were detected in this article.

Historical data was compared with the data in this study.

The change of different organics in the sediments around Beijing was concluded.

关键词： Organic compounds     Endocrine disrupters     Sediments     Concentration     Temporal changes    

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Mechanism and control factors of hydrate plugging in multiphase liquid-rich pipeline flow systems: a

Shuwei ZHANG, Liyan SHANG, Zhen PAN, Li ZHOU, You GUO

《能源前沿（英文）》 2022年 第16卷 第5期   页码 747-773 doi: 10.1007/s11708-022-0830-z

摘要： There is nothing illogical in the concept that hydrates are easily formed in oil and gas pipelines owing to the low-temperature and high-pressure environment, although requiring the cooperation of flow rate, water content, gas-liquid ratio, and other specific factors. Therefore, hydrate plugging is a major concern for the hydrate slurry pipeline transportation technology. In order to further examine potential mechanisms underlying these processes, the present paper listed and analyzed the significant research efforts specializing in the mechanisms of hydrate blockages in the liquid-rich system, including oil-based, water-based, and partially dispersed systems (PD systems), in gathering and transportation pipelines. In addition, it summarized the influences of fluid flow and water content on the risk of hydrate blockage and discussed. In general, flow rate was implicated in the regulation of blockage risk through its characteristic to affect sedimentation tendencies and flow patterns. Increasing water content can potentiate the growth of hydrates and change the oil-water dispersion degree, which causes a transition from completely dispersed systems to PD systems with a higher risk of clogging. Reasons of diversity of hydrate plugging mechanism in oil-based system ought to be studied in-depth by combining the discrepancy of water content and the microscopic characteristics of hydrate particles. At present, it is increasingly necessary to expand the application of the hydrate blockage formation prediction model in order to ensure that hydrate slurry mixed transportation technology can be more maturely applied to the natural gas industry transportation field.

关键词： hydrate     flow rate     water content     mechanism of pipeline blockage     rich liquid phase system    

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标题 作者 时间 类型 操作

Analysis of physical properties of gas hydrate-bearing unconsolidated sediment samples from the ultra-deepwater

期刊论文

Fundamental characteristics of gas hydrate-bearing sediments in the Shenhu area, South China Sea

Xin LYU, Qingping LI, Yang GE, Junlong ZHU, Shouwei ZHOU, Qiang FU

期刊论文

Research progress on hydrate plugging in multiphase mixed rich-liquid transportation pipelines

Shuyu SONG, Zhiming LIU, Li ZHOU, Liyan SHANG, Yaxin WANG

期刊论文

Adsorption and partition of benzo(a)pyrene on sediments with different particle sizes from the Yellow

XIA Xinghui, HU Lijuan, MENG Lihong

期刊论文

Prediction of bed load sediments using different artificial neural network models

Reza ASHEGHI, Seyed Abbas HOSSEINI

期刊论文

Progress in use of surfactant in nearly static conditions in natural gas hydrate formation

Zhen PAN, Yi WU, Liyan SHANG, Li ZHOU, Zhien ZHANG

期刊论文

Sorption of tetracycline to sediments and soils: assessing the roles of pH, the presence of cadmium andproperties of sediments and soils

Guixiang ZHANG, Xitao LIU, Ke SUN, Ye ZHAO, Chunye LIN

期刊论文

Impacts of CO2 and H2S on the risk of hydrate formation during pipeline transport of natural gas

Solomon A. Aromada, Bjørn Kvamme

期刊论文

in numerical simulations on multiphase flow and thermodynamics in production of natural gas from gas hydrate

Lin ZUO, Lixia SUN, Changfu YOU

期刊论文

Efficient promotion of methane hydrate formation and elimination of foam generation using fluorinated

Quan CAO, Dongyan XU, Huanfei XU, Shengjun LUO, Rongbo GUO

期刊论文

Progress and prospect of hydrate-based desalination technology

Jibao ZHANG, Shujun CHEN, Ning MAO, Tianbiao HE

期刊论文

Assessment on contaminations in sediments of an intake and the inflow canals in Taihu Lake, China

Xiaolong WANG,Shiming DING,Qi ZHANG,Weiping HU

期刊论文

Key issues in development of offshore natural gas hydrate

Shouwei ZHOU, Qingping LI, Xin LV, Qiang FU, Junlong ZHU

期刊论文

The temporal changes of the concentration level of typical toxic organics in the river sediments around

Qiang Li, Xiong Xu, Yaoyao Fang, Ruiyang Xiao, Donghong Wang, Wenjue Zhong

期刊论文

Mechanism and control factors of hydrate plugging in multiphase liquid-rich pipeline flow systems: a

Shuwei ZHANG, Liyan SHANG, Zhen PAN, Li ZHOU, You GUO

期刊论文